Gebruiksaanwijzing /service van het product 3000ZA van de fabrikant Teledyne
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Trace Oxygen Analyzer Teledyne Analytical Instruments i OPERA TING INSTRUCTIONS FOR MODEL 3000ZA T race Oxygen Analyzer DANGER Toxi c gases and or fl amm able l iquid s may be presen t in thi s mo nit orin g syste m. Personal protective equipment may be required when servicing this instrument.
3000ZA Teledyne Analytical Instruments ii Copyright © 2003 Teledyne Analytical Instruments A ll R ig h ts R e s e r ve d . N o pa r t of t hi s m an u a l m a y be r e pr odu c ed , tr a nsm i tt e d.
Trace Oxygen Analyzer Teledyne Analytical Instruments iii Specific Model Information The instrument for which this manual was supplied may incorporate one or more options not supplied in the standard instrument. Commonly available options are listed below, with check boxes.
3000ZA Teledyne Analytical Instruments iv Important Notice Model 3000ZA complies with all of the requirements of the Commonwealth of Europe (CE) for Radio Frequency Interference, Electromagnetic Interference (RFI/EMI), and Low Voltage Directive (LVD).
Trace Oxygen Analyzer Teledyne Analytical Instruments v Safety Messages Your safety and the safety of others is very important. We have provided many important safety messages in this manual. Please read these messages carefully. A safety message alerts you to potential hazards that could hurt you or others.
3000ZA Teledyne Analytical Instruments vi CAUTION: THE ANALYZER SHOULD ONLY BE USED FOR THE PURPOSE AND IN THE MANNER DESCRIBED IN THIS MANUAL. IF YOU USE THE ANALYZER IN A MANNER OTHER THAN THAT FOR WHICH IT WAS INTENDED, UNPREDICTABLE BEHAVIOR COULD RESULT POSSIBLY ACCOMPANIED WITH HAZARDOUS CONSEQUENCES.
Trace Oxygen Analyzer Teledyne Analytical Instruments vii This is a general purpose instrument designed for use in a non-hazardous area. It is the customer's responsibility to ensure safety especially when combustible gases are being analyzed since the potential of gas leaks always exist.
3000ZA Teledyne Analytical Instruments viii T able of Contents Safety Messages .......... ........... ............ ............ ........... ...... v 1.1 Overview 1 1.2 Typical Applications 1 1.3 Main Features of the Analyzer 1 1.4 Model Designations 2 1.
Trace Oxygen Analyzer Teledyne Analytical Instruments ix Operation ......... ............ ........... ............ ............ ........... .... 28 4.1 Introduction 28 4.2 Using the Data Entry and Function Buttons 29 4.3 The System Function 31 4.3.1 Tracking the Oxygen Readings during Calibration 32 4.
3000ZA Teledyne Analytical Instruments x 5.3 Fuse Replacement 53 5.4 System Self Diagnostic Test 54 5.5 Major Internal Components 55 5.6 Cleaning 56 5.7 Troubleshooting 56 Appendix ......... ............ ........... ............ ............ .........
Trace Oxygen Analyzer Teledyne Analytical Instruments xi List of Figures Figure 1-1: Model 3000ZA Front Panel 3 Figure 1-2: Model 3000ZA Rear Panel 5 Figure 2-1: Model 3000ZA Sample System 9 Figure 2-.
3000ZA Teledyne Analytical Instruments xii List of T ables Table 3-1: Analog Output Connections 20 Table 3-2: Alarm Relay Contact Pins 21 Table 3-3: Remote Calibration Connections 22 Table 3-4: Range .
Trace Oxygen Analyzer Introduction Teledyne Analytical Instruments 1 Introduction 1.1 Overview The Teledyne Analytical Instruments Model 3000ZA Trace Oxygen Analyzer is a versatile microprocessor-based instrument for detecting oxygen at the parts-per-million (ppm) level in a variety of gases.
Introduction 3000ZA Teledyne Analytical Instruments 2 offset and six months warranty and an expected lifetime of more than three years. 0-1 ppm range is possible too. • No reference gas required • Versatile analysis over a wide range of applications.
Trace Oxygen Analyzer Introduction Teledyne Analytical Instruments 3 3000ZA-M: This model has current output signals (4-20- mA) for ppm range and range ID, in addition to voltage outputs. 3000ZA-V: Gas flow through the cell block in this model is driven by vacuum downstream from the cell block instead of upstream pressure.
Introduction 3000ZA Teledyne Analytical Instruments 4 Function Keys: Six touch-sensitive membrane switches are used to change the specific function performed by the analyzer: • Analyze Perform analysis for oxygen content of a sample gas. • System Perform system-related tasks (described in detail in chapter 4, Operation.
Trace Oxygen Analyzer Introduction Teledyne Analytical Instruments 5 Standby Button : The Standby turns off the display and outputs but circuitry is still operating. CA UT ION: TH E POW ER CA B LE M UST B E UN PL U GGE D T O FU LL Y DIS CO NNE CT POWE R FR OM TH E INST RU MEN T.
Introduction 3000ZA Teledyne Analytical Instruments 6 • Power Connection Universal AC power source. • Ga s I nl e t a nd O utl e t O ne in l et ( mu s t be e xt e rna l ly va l ve d) a nd o n e ex h a us t o ut . Th re e in le ts w he n o p ti on “ C” i s o rd e re d.
Trace Oxygen Analyzer Introduction Teledyne Analytical Instruments 7 scheduled calibrations can vary 2-3 % per day..
Operational Theory 3000ZA Teledyne Analytical Instruments 8 Operational Theory 2.1 Introduction The analyzer is composed of three subsystems: 1. Zirconium Oxide (ZrO 2 ) Sensor 2.
Trace Oxygen Analyzer Operational Theory Teledyne Analytical Instruments 9 2.3 Sample System The sample system delivers gases to the ZrO 2 sensor from the analyzer rear panel inlet. Depending on the mode of operation either sample or calibration gas is delivered.
Operational Theory 3000ZA Teledyne Analytical Instruments 10 Figure 2-2: Flow Diagram with Options 2.4 Zirconium Oxide Sensor Application Notes The following sample gases require conditioning prior to entering the sensor: • Flammable gases such as methane, alcohol and carbon monoxide may cause a measurement error.
Trace Oxygen Analyzer Operational Theory Teledyne Analytical Instruments 11 The signal processing electronics including the microprocessor, analog to digital, and digital to analog converters are located on the motherboard at the bottom of the case. The preamplifier board is mounted on top of the motherboard as shown in the figure.
Operational Theory 3000ZA Teledyne Analytical Instruments 12 Figure 2-3: Component Location.
Trace Oxygen Analyzer Operational Theory Teledyne Analytical Instruments 13 Figure 2-4: Electronic Block Diagram.
Installation 3000ZA Teledyne Analytical Instruments 14 Installation Installation of the Model 3000ZA Analyzer includes: 1. Unpacking 2. Mounting 3. Gas connections 4.
Trace Oxygen Analyzer Installation Teledyne Analytical Instruments 15 Figure 3-1: Front Panel of the Model 3000TA (Model 3000ZA similar) All operator controls, except the flow control needle valve, ar.
Installation 3000ZA Teledyne Analytical Instruments 16 3.3 Rear Panel Connections Figure 3-3 shows the Model 3000ZA rear panel. There are ports for gas, power, and equipment interface. The Zero In and Span In ports are not included on the standard model but are available as options.
Trace Oxygen Analyzer Installation Teledyne Analytical Instruments 17 pressure applications (5-50 psig) use the restrictor that has a blue sticker on the body.
Installation 3000ZA Teledyne Analytical Instruments 18 If greater sample flow is required for improved response time, install a bypass in the sampling system upstream of the analyzer input. EXHAUST OUT: Exhaust connections must be consistent with the hazard level of the constituent gases.
Trace Oxygen Analyzer Installation Teledyne Analytical Instruments 19 Fuse Installation: The fuse block, at the right of the power cord receptacle, accepts US or European size fuses. A jumper replaces the fuse in whichever fuse receptacle is not used.
Installation 3000ZA Teledyne Analytical Instruments 20 Table 3-1: Analog Output Connections Pin Function 3 + Range ID, 4-20 mA, floating 4 – Range ID, 4-20 mA, floating 5 + ppm Range, 4-20 mA, float.
Trace Oxygen Analyzer Installation Teledyne Analytical Instruments 21 • Actuates when DC power supplied to circuits is unacceptable in one or more parameters. Permanently configured as failsafe and latching. Cannot be defeated. Actuates if self test fails.
Installation 3000ZA Teledyne Analytical Instruments 22 Span: Floating input. 5 to 24 V input across the + and – pins puts the analyzer into the Span mode. Either side may be grounded at the source of the signal. 0 to 1 volt across the terminals allows Span mode to terminate when done.
Trace Oxygen Analyzer Installation Teledyne Analytical Instruments 23 3. When CRC opens again, send a span command until the CRC closes. (The CRC will quickly close.) 4. When the CRC closes, remove the span command. When CRC opens again, zero and span are done, and the sample is being analyzed.
Installation 3000ZA Teledyne Analytical Instruments 24 Figure 3-5: Remote Probe Connections The voltage from these outputs is nominally 0 V for the OFF and 15 VDC for the ON conditions. The maximum combined current that can be pulled from these output lines is 100 mA.
Trace Oxygen Analyzer Installation Teledyne Analytical Instruments 25 3.3.2.3 RS-232 P ORT The digital signal output is a standard, full duplex RS-232 serial communications port used to connect the analyzer to a computer, terminal, or other digital device.
Installation 3000ZA Teledyne Analytical Instruments 26 Parity none Stop Bits 1 Message Interval 2 seconds. When CRC opens again, zero and span are done, and the sample is being analyzed. Range ID Relays: There are three dedicated Range ID relay contacts.
Trace Oxygen Analyzer Installation Teledyne Analytical Instruments 27 • Check the integrity and accuracy of the gas connections. Make sure there are no leaks. • Check the integrity and accuracy of the electrical connections. Make sure there are no exposed conductors.
Operation 3000ZA Teledyne Analytical Instruments 28 Operation 4.1 Introduction Once the analyzer has been installed, it can be configured for your application. To do this you will: • Set system parameters. • Establish a security password, if desired, requiring Operator to log in.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 29 4.2 Using the Data Entry and Function Buttons Data Entry Buttons: The __ arrow buttons select options from the menu currently being displayed on the VFD screen. The selected option blinks.
Operation 3000ZA Teledyne Analytical Instruments 30 Figure 4-1: Hierarchy of Available Functions Any function can be selected at any time by pressing the appropriate button (unless password restrictions apply). The order as presented in this manual is appropriate for an initial setup.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 31 4.3 The System Function The sub fuctions of the System function are described below. Specific procedures for their use follow the descriptions: • Auto-Cal: Used to define an automatic calibration sequence and/or start an Auto-Cal.
Operation 3000ZA Teledyne Analytical Instruments 32 4.3.1 Tracking the Oxygen Readings during Calibration and Alarm delay The user has the option of setting the preference as to whether the analog outputs track the display readings during calibration or not.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 33 The factory default is three minutes, but the delay time is programmable. To adjust to delay time use the Left or Right arrow keys. When the time displayed on the second line blinks, it can be adjusted by Pressing the Up or Down keys to increase or decrease its value.
Operation 3000ZA Teledyne Analytical Instruments 34 Zero) OFF/ON field. Use __ arrows to set the OFF/ON field to ON. You can now turn these fields ON because there is a nonzero span interval defined.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 35 The screen prompts you to enter the current password. If you are not using password protection, press Enter to accept TETAI as the default password.
Operation 3000ZA Teledyne Analytical Instruments 36 Enter the password using the __ arrow keys to move back and forth between the existing password letters, and the __ arrow keys to change the letters to the new password. The full set of 94 characters available for password use are shown in the table below.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 37 If an alarm is tripped, the second line will change to show which alarm it is: 0.0 ppm Anlz AL—1 Note: If you log off the system us.
Operation 3000ZA Teledyne Analytical Instruments 38 TRAK/HLD Auto—Cal PSWD Logout More Use the __ arrow keys to blink More , then press Enter . Version Self—Test Use the __ arrow keys again to move the blinking to the Self–Test function. The screen will follow the running of the diagnostic.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 39 TRAK/HLD Auto—Cal PSWD Logout More Use the __ arrow keys to blink More , then press Enter . Version Self—Test Show_Negative=NO Use the __ arrow keys and select “ Show_Negative = NO”.
Operation 3000ZA Teledyne Analytical Instruments 40 If you are using password protection, you will need to enter your password to gain access to either of these functions. Follow the instructions in sections 4.3.3 to enter your password. Once you have gained clearance to proceed, you can enter the Zero or Span function.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 41 The zeroing process will automatically conclude when the output is within the acceptable range for a good zero. Then the analyzer automatically returns to the Analyze mode. 4.4.1.2 M ANUAL M ODE Z EROING Press Zero to enter the Zero function.
Operation 3000ZA Teledyne Analytical Instruments 42 CELL FAIL/ ZERO HIGH Before replacing the cell: a. Check your span gas to make sure it is within specifications. b. Check for leaks up-stream from the cell, where oxygen may be leaking into the system.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 43 Use the __ arrow keys to enter the oxygen-concentration mode. Use the __ arrow keys to blink the digit you are going to modify. Use the __ arrow keys again to change the value of the selected digit.
Operation 3000ZA Teledyne Analytical Instruments 44 Press Enter to enter the span value into the system and begin the span calibration. Once the span has begun, the microprocessor samples the output at a predetermined rate. It calculates the difference between successive samplings and displays this difference as a Slope on the screen.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 45 4.5 The Alarms Function The Model 3000ZA is equipped with 2 fully adjustable concentration alarms and a system failure alarm. Each alarm has a relay with a set of form “C" contacts rated for 3 amperes resistive load at 250 VAC.
Operation 3000ZA Teledyne Analytical Instruments 46 back to non-alarm conditions. This mode requires an alarm to be recognized before it can be reset. In the non-latching mode, the alarm status will terminate when process conditions revert to non-alarm conditions.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 47 To set the other parameters use the __ arrow keys to move the blinking over to the desired parameter. Then use the __ arrow keys to change the parameter. Once the parameters for alarm 1 have been set, press Alarms again, and repeat this procedure for alarm 2 ( AL–2 ).
Operation 3000ZA Teledyne Analytical Instruments 48 L—10 M—100 H—250 Mode—AUTO Use the __ arrow keys to blink the range to be set: low (L), medium (M), or high (H). Use the __ arrow keys to enter the upper value of the range (all ranges begin at 0 ppm).
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 49 as established by the operator for that particular range, the output saturates at 1 VDC(or 20 mA). However, the digital readout and the RS-232 output continue to read the true value of the oxygen concentration regardless of the analog output range.
Operation 3000ZA Teledyne Analytical Instruments 50 80 0.8 16.8 90 0.9 18.4 100 1.0 20.0 The analog output signal has a voltage which depends on the oxygen concentration AND the currently activated analysis range.
Trace Oxygen Analyzer Operation Teledyne Analytical Instruments 51.
Maintenance 3000ZA Teledyne Analytical Instruments 52 Maintenance 5.1 Routine Maintenance Aside from normal cleaning and checking for leaks at the gas connections, routine maintenance is limited to replacing the sensor and fuses, and recalibration. For recalibration, see Section 4.
Trace Oxygen Analyzer Maintenance Teledyne Analytical Instruments 53 4. Remove the old sensor and install a new sensor by matching the orientation notch on the sensor to the silkscreen on the sensor holder. Figure 5-1: Replacing the ZrO 2 Sensor 5.3 Fuse Replacement 1.
Maintenance 3000ZA Teledyne Analytical Instruments 54 2. To change between American and European fuses, remove the single retaining screw, flip Fuse Block over 180 degrees, and replace screw. 3. Replace fuse as shown in Figure 5-3. 4. Reassemble Housing as shown in Figure 5-2.
Trace Oxygen Analyzer Maintenance Teledyne Analytical Instruments 55 Preamp 0 OK 1 Zero too high 2 Amplifier output doesn't match test input 3 Both Failed 5.5 Major Internal Components The zirconium sensor is accessed by unlatching and swinging open the front panel, as described earlier.
Maintenance 3000ZA Teledyne Analytical Instruments 56 • Analysis Section • Zirconium oxide sensor • Cell block • Sample system • Power Supply • Microprocessor • Displays • 5 digit LED .
Trace Oxygen Analyzer Maintenance Teledyne Analytical Instruments 57 analyzer. 2. If erratic behavior continues, replace sensor. Atmospheric oxygen diffusing through vent and altering the oxygen level the sensor sees Increase flow rate and/or length of vent tubing to dilute or minimize oxygen diffusion from vent to sensor.
Appendix 3000ZA Teledyne Analytical Instruments Appendix A-1 Specifications Packaging: General Purpose • Flush panel mount (Standard) • Relay rack mount. Contains either one or two instruments in one 19" relay rack mountable plate (Optional).
Trace Oxygen Analyzer Appendix Teledyne Analytical Instruments Power: Universal power supply 85-250 V ac, at 47-63 Hz. Operating Temperature: 5-35 °C Accuracy: ±2% of full scale at constant temperature (at ca;obrated ramge). ±5% of full scale over operating temperature range, except 0-1 ppm analysis range, once thermal equilibrium is reached.
Appendix 3000ZA Teledyne Analytical Instruments A-2 Recommended 2-Y ear Spare Parts List Qty. Part Number Description 1 C65507A Back Panel Board 1 C62371-A Front Panel Board 1 C75734A Trace Preamplifi.
Trace Oxygen Analyzer Appendix Teledyne Analytical Instruments A-3 Drawing List D-75739 Final Assembly D-75738 Outline Drawing A-4 19-inch Relay Rack Panel Mount Figure A-1: Single and Dual 19" R.
Appendix 3000ZA Teledyne Analytical Instruments A.5 Application Notes 3000 SERIES ANALYZERS APPLICATION NOTES ON RESTRICTORS, PRESSURES, AND FLOW RECOMMENDATIONS The 3000 series analyzers require reasonably regulated sample pressures.
Trace Oxygen Analyzer Appendix Teledyne Analytical Instruments positive pressure applications as well as vacuum service applications (see manual for installation instructions). The standard restrictor (BLUE DOT) is recommended for pressures between 5 and 50 PSIG.
Appendix 3000ZA Teledyne Analytical Instruments To imp r ov e the s ys tem res pon se, a by-pa s s can b e add ed to inc rea se the sa mple flo w ra te to the a naly zer by a fac tor o f ten. A by-pa ss provide s a s amp le flow pa th arou nd the ana lyzer of 2 - 18 SCF H.
Trace Oxygen Analyzer Appendix Teledyne Analytical Instruments 1 SCFH = 0.476 SLPM.
Index 3000ZA Teledyne Analytical Instruments Index AC power connection, 6 accuracy, 58 address, 59 alarm, 57 concentration, 2, 6, 44 configuration, 44 freeze, 31 relay contact pins, 20 relays, 19 setp.
Trace Oxygen Analyzer Index Teledyne Analytical Instruments exhaust out, 16, 17 external control, 6 external valves, 22 failsafe, 44 failure codes, 53 features, 1 FET, 23 fixed range, 46, 47 flow rang.
Index 3000ZA Teledyne Analytical Instruments relay connections, 22 relay contacts, 22 range ID contact, 6 range ID relay contacts, 25 range identification, 2 RANGE key, 28 readout, 4 rear panel, 5, 15 rear panel removal, 54 recovery, 49 remote calibration connections.
Trace Oxygen Analyzer Index Teledyne Analytical Instruments.
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